Nanostructured titanium dioxide film preparation using inorganic nanoparticles instead of organic precursor materials.

Carbon dioxide is a major contributor to global warming. A promising method of reducing the concentration of atmospheric carbon dioxide is by photocatalytic conversion of carbon dioxide into renewable fuels, which has to be done using a photocatalytic film. The nanostructured film preparation method...

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Main Authors: Jamali, A., Eghbali, M. H.
Format: Article
Language:Spanish
Published: Universidad Autónoma de Nuevo León 2011
Subjects:
Online Access:https://quimicahoy.uanl.mx/index.php/r/article/view/132
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author Jamali, A.
Eghbali, M. H.
author_facet Jamali, A.
Eghbali, M. H.
author_sort Jamali, A.
collection Artículos de Revistas UANL
description Carbon dioxide is a major contributor to global warming. A promising method of reducing the concentration of atmospheric carbon dioxide is by photocatalytic conversion of carbon dioxide into renewable fuels, which has to be done using a photocatalytic film. The nanostructured film preparation method proposed in this study is a preparation of colloidal solution followed by film deposition using manual coating methods, mostly vertical dip-coating. Deposited films were calcined to forma crystalline film on the glass substrate. This method was adopted in case of film preparation from titanium dioxide. Comprehensive study on impact of different factors including temperature, type of surfactants, type of solvents, concentration of surfactants, and concentration of solvents on quality of thin film including band gap, particle size, strength and homogeneity was performed in this work. Material characterisation tests including UV-visible spectroscopy and field emission scanning electron microscopy were carried out to analyse the film characteristics. Mechanical tests including wipe test, rinse test, acetone test, scratch test and scotch tape test were performed to analyse the mechanical strength of obtained thin film. Nanostructured films were successfully prepared with controlled particle size in the range of 70 - 100 nm for TiO2. Films obtained in this study demonstrate acceptable durability and partial uniformity. The film preparation method used in this study was markedly economical, facile and reproducible.
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physical Quimica Hoy; Vol. 1 No. 4 (2011): Julio-Septiembre 2011; 9-18
Quimica Hoy; Vol. 1 Núm. 4 (2011): Julio-Septiembre 2011; 9-18
2007-1183
publishDate 2011
publisher Universidad Autónoma de Nuevo León
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spelling quimicahoy-article-1322021-10-29T11:17:34Z Nanostructured titanium dioxide film preparation using inorganic nanoparticles instead of organic precursor materials. Jamali, A. Eghbali, M. H. Titanium dioxide nanostructured film preparation photocatalytic film Carbon dioxide is a major contributor to global warming. A promising method of reducing the concentration of atmospheric carbon dioxide is by photocatalytic conversion of carbon dioxide into renewable fuels, which has to be done using a photocatalytic film. The nanostructured film preparation method proposed in this study is a preparation of colloidal solution followed by film deposition using manual coating methods, mostly vertical dip-coating. Deposited films were calcined to forma crystalline film on the glass substrate. This method was adopted in case of film preparation from titanium dioxide. Comprehensive study on impact of different factors including temperature, type of surfactants, type of solvents, concentration of surfactants, and concentration of solvents on quality of thin film including band gap, particle size, strength and homogeneity was performed in this work. Material characterisation tests including UV-visible spectroscopy and field emission scanning electron microscopy were carried out to analyse the film characteristics. Mechanical tests including wipe test, rinse test, acetone test, scratch test and scotch tape test were performed to analyse the mechanical strength of obtained thin film. Nanostructured films were successfully prepared with controlled particle size in the range of 70 - 100 nm for TiO2. Films obtained in this study demonstrate acceptable durability and partial uniformity. The film preparation method used in this study was markedly economical, facile and reproducible. Universidad Autónoma de Nuevo León 2011-09-30 info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion Peer review articles Articulos evaluados por pares application/pdf https://quimicahoy.uanl.mx/index.php/r/article/view/132 10.29105/qh1.4-132 Quimica Hoy; Vol. 1 No. 4 (2011): Julio-Septiembre 2011; 9-18 Quimica Hoy; Vol. 1 Núm. 4 (2011): Julio-Septiembre 2011; 9-18 2007-1183 spa https://quimicahoy.uanl.mx/index.php/r/article/view/132/100 Derechos de autor 2011 A. Jamali, M. H. Eghbali https://creativecommons.org/licenses/by/4.0
spellingShingle Titanium dioxide
nanostructured film preparation
photocatalytic film
Jamali, A.
Eghbali, M. H.
Nanostructured titanium dioxide film preparation using inorganic nanoparticles instead of organic precursor materials.
thumbnail https://rediab.uanl.mx/themes/sandal5/images/article.gif
title Nanostructured titanium dioxide film preparation using inorganic nanoparticles instead of organic precursor materials.
title_full Nanostructured titanium dioxide film preparation using inorganic nanoparticles instead of organic precursor materials.
title_fullStr Nanostructured titanium dioxide film preparation using inorganic nanoparticles instead of organic precursor materials.
title_full_unstemmed Nanostructured titanium dioxide film preparation using inorganic nanoparticles instead of organic precursor materials.
title_short Nanostructured titanium dioxide film preparation using inorganic nanoparticles instead of organic precursor materials.
title_sort nanostructured titanium dioxide film preparation using inorganic nanoparticles instead of organic precursor materials
topic Titanium dioxide
nanostructured film preparation
photocatalytic film
topic_facet Titanium dioxide
nanostructured film preparation
photocatalytic film
url https://quimicahoy.uanl.mx/index.php/r/article/view/132
work_keys_str_mv AT jamalia nanostructuredtitaniumdioxidefilmpreparationusinginorganicnanoparticlesinsteadoforganicprecursormaterials
AT eghbalimh nanostructuredtitaniumdioxidefilmpreparationusinginorganicnanoparticlesinsteadoforganicprecursormaterials