Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description

The aim of this work is to present some results of the synthesis of nanoparticles of zinc oxide by means of a hydrothermal method. Also, a description of the structural characteristics of these nanoparticles will be presented. The nanoparticles can be used as the supported active phase for photocata...

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Autores principales: García Ruiz, Armando, Escobedo, A., Aguilar Hernández, Alberto Issac, Esparza, Rodrigo, Pérez, R.
Formato: Artículo
Lenguaje:Spanish / Castilian
Publicado: Universidad Autónoma de Puebla 2011
Materias:
Acceso en línea:http://eprints.uanl.mx/13445/1/Art5.pdf
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author García Ruiz, Armando
Escobedo, A.
Aguilar Hernández, Alberto Issac
Esparza, Rodrigo
Pérez, R.
author_facet García Ruiz, Armando
Escobedo, A.
Aguilar Hernández, Alberto Issac
Esparza, Rodrigo
Pérez, R.
author_sort García Ruiz, Armando
collection Repositorio Institucional
description The aim of this work is to present some results of the synthesis of nanoparticles of zinc oxide by means of a hydrothermal method. Also, a description of the structural characteristics of these nanoparticles will be presented. The nanoparticles can be used as the supported active phase for photocatalytic applications, as has been recently published in the literature. The hydrothermal synthesis is based in dehydrated zinc acetate as the precursor using temperatures of 100ºC. The structural analysis of the obtained nanoparticles has been performed using X-ray diffraction techniques with a subsequent Rietveld refinement of the pattern. This allows obtaining refined values of the cell parameters and the aproximate crystallite sizes (10-20 nm) and also gives an insight on the morphology of the nanoparticle (truncated cube). Some high resolution electron microscope images are also presented and their structural results are compared with those obtained through the X-ray diffraction stuides.
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spelling eprints-134452020-04-28T17:43:42Z http://eprints.uanl.mx/13445/ Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description García Ruiz, Armando Escobedo, A. Aguilar Hernández, Alberto Issac Esparza, Rodrigo Pérez, R. QD Química The aim of this work is to present some results of the synthesis of nanoparticles of zinc oxide by means of a hydrothermal method. Also, a description of the structural characteristics of these nanoparticles will be presented. The nanoparticles can be used as the supported active phase for photocatalytic applications, as has been recently published in the literature. The hydrothermal synthesis is based in dehydrated zinc acetate as the precursor using temperatures of 100ºC. The structural analysis of the obtained nanoparticles has been performed using X-ray diffraction techniques with a subsequent Rietveld refinement of the pattern. This allows obtaining refined values of the cell parameters and the aproximate crystallite sizes (10-20 nm) and also gives an insight on the morphology of the nanoparticle (truncated cube). Some high resolution electron microscope images are also presented and their structural results are compared with those obtained through the X-ray diffraction stuides. Universidad Autónoma de Puebla 2011-09-10 Article PeerReviewed text es cc_by_nc_nd http://eprints.uanl.mx/13445/1/Art5.pdf http://eprints.uanl.mx/13445/1.haspreviewThumbnailVersion/Art5.pdf García Ruiz, Armando y Escobedo, A. y Aguilar Hernández, Alberto Issac y Esparza, Rodrigo y Pérez, R. (2011) Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description. Química Hoy, 1 (4). pp. 24-28. ISSN 2007-1183
spellingShingle QD Química
García Ruiz, Armando
Escobedo, A.
Aguilar Hernández, Alberto Issac
Esparza, Rodrigo
Pérez, R.
Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
thumbnail https://rediab.uanl.mx/themes/sandal5/images/online.png
title Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
title_full Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
title_fullStr Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
title_full_unstemmed Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
title_short Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
title_sort hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
topic QD Química
url http://eprints.uanl.mx/13445/1/Art5.pdf
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