Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description

The aim of this work is to present some results of the synthesis of nanoparticles of zinc oxide by means of a hydrothermal method. Also, a description of the structural characteristics of these nanoparticles will be presented. The nanoparticles can be used as the supported active phase for photocata...

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Autores principales: García Ruiz, A., Escobedo, A., Aguilar, A., Esparza, R., Pérez, R.
Formato: Artículo
Lenguaje:inglés
Publicado: Universidad Autónoma de Nuevo León 2011
Materias:
Acceso en línea:https://quimicahoy.uanl.mx/index.php/r/article/view/138
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author García Ruiz, A.
Escobedo, A.
Aguilar, A.
Esparza, R.
Pérez, R.
author_facet García Ruiz, A.
Escobedo, A.
Aguilar, A.
Esparza, R.
Pérez, R.
author_sort García Ruiz, A.
collection Artículos de Revistas UANL
description The aim of this work is to present some results of the synthesis of nanoparticles of zinc oxide by means of a hydrothermal method. Also, a description of the structural characteristics of these nanoparticles will be presented. The nanoparticles can be used as the supported active phase for photocatalytic applications, as has been recently published in the literature. The hydrotbermal synthesis is based in dehydrated zinc acetate as the precursor using temperatures of 100ºC. The structural analysis of the obtained nanoparticles has been performed using X-ray diffraction techniques with a subsequent Rietveld refinement of the pattern. This allows obtaining refined values of the cell parameters and the approximate crystallite sizes (10-20 nm) and also gives an insight on the morphology of the nanoparticle (truncated cube). Some high resolution electron microscope images are also presented and their structural results are compared with those obtained through the X-ray diffraction studies.
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physical Quimica Hoy; Vol. 1 No. 4 (2011): Julio-Septiembre 2011; 24-28
Quimica Hoy; Vol. 1 Núm. 4 (2011): Julio-Septiembre 2011; 24-28
2007-1183
publishDate 2011
publisher Universidad Autónoma de Nuevo León
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spelling quimicahoy-article-1382021-10-29T11:17:34Z Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description García Ruiz, A. Escobedo, A. Aguilar, A. Esparza, R. Pérez, R. Nanostructured oxides hydrothermal synthesis crystal structure X-ray diffraction (XRD) transmission electron microscopy (TEM) crystallite morphology The aim of this work is to present some results of the synthesis of nanoparticles of zinc oxide by means of a hydrothermal method. Also, a description of the structural characteristics of these nanoparticles will be presented. The nanoparticles can be used as the supported active phase for photocatalytic applications, as has been recently published in the literature. The hydrotbermal synthesis is based in dehydrated zinc acetate as the precursor using temperatures of 100ºC. The structural analysis of the obtained nanoparticles has been performed using X-ray diffraction techniques with a subsequent Rietveld refinement of the pattern. This allows obtaining refined values of the cell parameters and the approximate crystallite sizes (10-20 nm) and also gives an insight on the morphology of the nanoparticle (truncated cube). Some high resolution electron microscope images are also presented and their structural results are compared with those obtained through the X-ray diffraction studies. Universidad Autónoma de Nuevo León 2011-09-30 info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion Peer review articles Articulos evaluados por pares application/pdf https://quimicahoy.uanl.mx/index.php/r/article/view/138 10.29105/qh1.4-138 Quimica Hoy; Vol. 1 No. 4 (2011): Julio-Septiembre 2011; 24-28 Quimica Hoy; Vol. 1 Núm. 4 (2011): Julio-Septiembre 2011; 24-28 2007-1183 eng https://quimicahoy.uanl.mx/index.php/r/article/view/138/106 Derechos de autor 2011 A. García Ruiz, A. Escobedo, A. Aguilar, R. Esparza, R. Pérez https://creativecommons.org/licenses/by/4.0
spellingShingle Nanostructured oxides
hydrothermal synthesis
crystal structure
X-ray diffraction (XRD)
transmission electron microscopy (TEM)
crystallite morphology
García Ruiz, A.
Escobedo, A.
Aguilar, A.
Esparza, R.
Pérez, R.
Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
thumbnail https://rediab.uanl.mx/themes/sandal5/images/article.gif
title Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
title_full Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
title_fullStr Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
title_full_unstemmed Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
title_short Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
title_sort hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
topic Nanostructured oxides
hydrothermal synthesis
crystal structure
X-ray diffraction (XRD)
transmission electron microscopy (TEM)
crystallite morphology
topic_facet Nanostructured oxides
hydrothermal synthesis
crystal structure
X-ray diffraction (XRD)
transmission electron microscopy (TEM)
crystallite morphology
url https://quimicahoy.uanl.mx/index.php/r/article/view/138
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