Microwave-assisted synthesis and characterization of microstar shaped zinc oxide
A microwave-assisted solution-phase approach has been applied for the synthesis of zinc oxide microstructures. The synthesis procedure was carried out byusing tbe reagents: Zinc nitrate and Methenamine, at stoichiometric ratio. AnaIysis by means ofX-ray Diffraction (XRD) shows a crystalline phase in...
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| Format: | Article |
| Language: | English |
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2012
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| Online Access: | http://eprints.uanl.mx/3119/1/Art3.pdf |
| _version_ | 1836397372993699840 |
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| author | Palomar Pérez, Flor Esthela Yacamán, Miguel José Gómez de la Fuente, María Idalia del Consuelo |
| author_facet | Palomar Pérez, Flor Esthela Yacamán, Miguel José Gómez de la Fuente, María Idalia del Consuelo |
| author_sort | Palomar Pérez, Flor Esthela |
| collection | Repositorio Institucional |
| description | A microwave-assisted solution-phase approach has been applied for the synthesis of zinc oxide microstructures. The synthesis procedure was carried out byusing tbe reagents: Zinc nitrate and Methenamine, at stoichiometric ratio. AnaIysis by means ofX-ray Diffraction (XRD) shows a crystalline phase in hexagonal wurtzite arrangement for ZnO. The presence ofmicrostar shaped zinc oxide (2-3Jlm) with nanorods-{5Onm) arranged has been confirmed from High Resolution Scanning Electron Microscopy (HRSEM). The formation ofnanorods was confirmed by Transmission Electron Microscopy. In Raman spectros copy a red shift was detected in the microstructures compared with Zno bulk. High crystalline materials witbout additional post-syn.thesis treatment were found. |
| format | Article |
| id | eprints-3119 |
| institution | UANL |
| language | English |
| publishDate | 2012 |
| record_format | eprints |
| spelling | eprints-31192025-06-27T18:25:29Z http://eprints.uanl.mx/3119/ Microwave-assisted synthesis and characterization of microstar shaped zinc oxide Palomar Pérez, Flor Esthela Yacamán, Miguel José Gómez de la Fuente, María Idalia del Consuelo Q Ciencias en General QD Química A microwave-assisted solution-phase approach has been applied for the synthesis of zinc oxide microstructures. The synthesis procedure was carried out byusing tbe reagents: Zinc nitrate and Methenamine, at stoichiometric ratio. AnaIysis by means ofX-ray Diffraction (XRD) shows a crystalline phase in hexagonal wurtzite arrangement for ZnO. The presence ofmicrostar shaped zinc oxide (2-3Jlm) with nanorods-{5Onm) arranged has been confirmed from High Resolution Scanning Electron Microscopy (HRSEM). The formation ofnanorods was confirmed by Transmission Electron Microscopy. In Raman spectros copy a red shift was detected in the microstructures compared with Zno bulk. High crystalline materials witbout additional post-syn.thesis treatment were found. 2012 Article PeerReviewed application/pdf en cc_by_nc_nd http://eprints.uanl.mx/3119/1/Art3.pdf http://eprints.uanl.mx/3119/1.haspreviewThumbnailVersion/Art3.pdf Palomar Pérez, Flor Esthela y Yacamán, Miguel José y Gómez de la Fuente, María Idalia del Consuelo (2012) Microwave-assisted synthesis and characterization of microstar shaped zinc oxide. Química Hoy, 2 (3). |
| spellingShingle | Q Ciencias en General QD Química Palomar Pérez, Flor Esthela Yacamán, Miguel José Gómez de la Fuente, María Idalia del Consuelo Microwave-assisted synthesis and characterization of microstar shaped zinc oxide |
| thumbnail | https://rediab.uanl.mx/themes/sandal5/images/online.png |
| title | Microwave-assisted synthesis and characterization of microstar shaped zinc oxide |
| title_full | Microwave-assisted synthesis and characterization of microstar shaped zinc oxide |
| title_fullStr | Microwave-assisted synthesis and characterization of microstar shaped zinc oxide |
| title_full_unstemmed | Microwave-assisted synthesis and characterization of microstar shaped zinc oxide |
| title_short | Microwave-assisted synthesis and characterization of microstar shaped zinc oxide |
| title_sort | microwave assisted synthesis and characterization of microstar shaped zinc oxide |
| topic | Q Ciencias en General QD Química |
| url | http://eprints.uanl.mx/3119/1/Art3.pdf |
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