Green Synthesis of Magnetic Nanoparticles of Iron Oxide Using Aqueous Extracts of Lemon Peel Waste and Its Application in Anti-Corrosive Coatings

Lately, the development of green chemistry methods with high efficiency for metal nanoparticle synthesis has become a primary focus among researchers. The main goal is to find an eco-friendly technique for the production of nanoparticles. Ferro- and ferrimagnetic materials such as magnetite (Fe3O4)...

Descripción completa

Detalles Bibliográficos
Autores principales: Elizondo Villarreal, Nora, Verástegui Domínguez, Luz Hypatia, Rodríguez Batista, Raúl, Gándara Martínez, Eleazar, Alcorta García, Aracelia, Martínez Delgado, Dora Irma, Rodríguez Castellanos, Edén Amaral, Vázquez Rodríguez, Francisco Javier, Gómez Rodríguez, Cristian
Formato: Artículo
Lenguaje:inglés
Publicado: Molecular Diversity Preservation International 2022
Materias:
Acceso en línea:http://eprints.uanl.mx/26210/1/26210.pdf
_version_ 1824420440822513664
author Elizondo Villarreal, Nora
Verástegui Domínguez, Luz Hypatia
Rodríguez Batista, Raúl
Gándara Martínez, Eleazar
Alcorta García, Aracelia
Martínez Delgado, Dora Irma
Rodríguez Castellanos, Edén Amaral
Vázquez Rodríguez, Francisco Javier
Gómez Rodríguez, Cristian
author_facet Elizondo Villarreal, Nora
Verástegui Domínguez, Luz Hypatia
Rodríguez Batista, Raúl
Gándara Martínez, Eleazar
Alcorta García, Aracelia
Martínez Delgado, Dora Irma
Rodríguez Castellanos, Edén Amaral
Vázquez Rodríguez, Francisco Javier
Gómez Rodríguez, Cristian
author_sort Elizondo Villarreal, Nora
collection Repositorio Institucional
description Lately, the development of green chemistry methods with high efficiency for metal nanoparticle synthesis has become a primary focus among researchers. The main goal is to find an eco-friendly technique for the production of nanoparticles. Ferro- and ferrimagnetic materials such as magnetite (Fe3O4) exhibit superparamagnetic behavior at a nanometric scale. Magnetic nanoparticles have been gaining increasing interest in nanoscience and nanotechnology. This interest is attributed to their physicochemical properties, particle size, and low toxicity. The present work aims to synthesize magnetite nanoparticles in a single step using extracts of green lemon Citrus Aurantifolia residues. The results produced nanoparticles of smaller size using a method that is friendlier to health and the environment, is more profitable, and can be applied in anticorrosive coatings. The green synthesis was carried out by a co-precipitation method under variable temperature conditions. The X-ray Diffraction (XRD) and Transmission Electron Microscopy (TEM) characterization showed that magnetite nanoparticles were successfully obtained with a very narrow particle size distribution between 3 and 10 nm. A composite was produced with the nanoparticles and graphene to be used as a surface coating on steel. In addition, the coating’s anticorrosive behavior was evaluated through electrochemical techniques. The surface coating obtained showed good anticorrosive properties and resistance to abrasion.
format Article
id eprints-26210
institution UANL
language English
publishDate 2022
publisher Molecular Diversity Preservation International
record_format eprints
spelling eprints-262102023-09-21T16:44:24Z http://eprints.uanl.mx/26210/ Green Synthesis of Magnetic Nanoparticles of Iron Oxide Using Aqueous Extracts of Lemon Peel Waste and Its Application in Anti-Corrosive Coatings Elizondo Villarreal, Nora Verástegui Domínguez, Luz Hypatia Rodríguez Batista, Raúl Gándara Martínez, Eleazar Alcorta García, Aracelia Martínez Delgado, Dora Irma Rodríguez Castellanos, Edén Amaral Vázquez Rodríguez, Francisco Javier Gómez Rodríguez, Cristian TA Ingeniería General y Civil Lately, the development of green chemistry methods with high efficiency for metal nanoparticle synthesis has become a primary focus among researchers. The main goal is to find an eco-friendly technique for the production of nanoparticles. Ferro- and ferrimagnetic materials such as magnetite (Fe3O4) exhibit superparamagnetic behavior at a nanometric scale. Magnetic nanoparticles have been gaining increasing interest in nanoscience and nanotechnology. This interest is attributed to their physicochemical properties, particle size, and low toxicity. The present work aims to synthesize magnetite nanoparticles in a single step using extracts of green lemon Citrus Aurantifolia residues. The results produced nanoparticles of smaller size using a method that is friendlier to health and the environment, is more profitable, and can be applied in anticorrosive coatings. The green synthesis was carried out by a co-precipitation method under variable temperature conditions. The X-ray Diffraction (XRD) and Transmission Electron Microscopy (TEM) characterization showed that magnetite nanoparticles were successfully obtained with a very narrow particle size distribution between 3 and 10 nm. A composite was produced with the nanoparticles and graphene to be used as a surface coating on steel. In addition, the coating’s anticorrosive behavior was evaluated through electrochemical techniques. The surface coating obtained showed good anticorrosive properties and resistance to abrasion. Molecular Diversity Preservation International 2022 Article PeerReviewed text en cc_by_nc_nd http://eprints.uanl.mx/26210/1/26210.pdf http://eprints.uanl.mx/26210/1.haspreviewThumbnailVersion/26210.pdf Elizondo Villarreal, Nora y Verástegui Domínguez, Luz Hypatia y Rodríguez Batista, Raúl y Gándara Martínez, Eleazar y Alcorta García, Aracelia y Martínez Delgado, Dora Irma y Rodríguez Castellanos, Edén Amaral y Vázquez Rodríguez, Francisco Javier y Gómez Rodríguez, Cristian (2022) Green Synthesis of Magnetic Nanoparticles of Iron Oxide Using Aqueous Extracts of Lemon Peel Waste and Its Application in Anti-Corrosive Coatings. Materials, 15 (23). pp. 1-22. ISSN 1996-1944 http://doi.org/10.3390/ma15238328 doi:10.3390/ma15238328
spellingShingle TA Ingeniería General y Civil
Elizondo Villarreal, Nora
Verástegui Domínguez, Luz Hypatia
Rodríguez Batista, Raúl
Gándara Martínez, Eleazar
Alcorta García, Aracelia
Martínez Delgado, Dora Irma
Rodríguez Castellanos, Edén Amaral
Vázquez Rodríguez, Francisco Javier
Gómez Rodríguez, Cristian
Green Synthesis of Magnetic Nanoparticles of Iron Oxide Using Aqueous Extracts of Lemon Peel Waste and Its Application in Anti-Corrosive Coatings
thumbnail https://rediab.uanl.mx/themes/sandal5/images/online.png
title Green Synthesis of Magnetic Nanoparticles of Iron Oxide Using Aqueous Extracts of Lemon Peel Waste and Its Application in Anti-Corrosive Coatings
title_full Green Synthesis of Magnetic Nanoparticles of Iron Oxide Using Aqueous Extracts of Lemon Peel Waste and Its Application in Anti-Corrosive Coatings
title_fullStr Green Synthesis of Magnetic Nanoparticles of Iron Oxide Using Aqueous Extracts of Lemon Peel Waste and Its Application in Anti-Corrosive Coatings
title_full_unstemmed Green Synthesis of Magnetic Nanoparticles of Iron Oxide Using Aqueous Extracts of Lemon Peel Waste and Its Application in Anti-Corrosive Coatings
title_short Green Synthesis of Magnetic Nanoparticles of Iron Oxide Using Aqueous Extracts of Lemon Peel Waste and Its Application in Anti-Corrosive Coatings
title_sort green synthesis of magnetic nanoparticles of iron oxide using aqueous extracts of lemon peel waste and its application in anti corrosive coatings
topic TA Ingeniería General y Civil
url http://eprints.uanl.mx/26210/1/26210.pdf
work_keys_str_mv AT elizondovillarrealnora greensynthesisofmagneticnanoparticlesofironoxideusingaqueousextractsoflemonpeelwasteanditsapplicationinanticorrosivecoatings
AT verasteguidominguezluzhypatia greensynthesisofmagneticnanoparticlesofironoxideusingaqueousextractsoflemonpeelwasteanditsapplicationinanticorrosivecoatings
AT rodriguezbatistaraul greensynthesisofmagneticnanoparticlesofironoxideusingaqueousextractsoflemonpeelwasteanditsapplicationinanticorrosivecoatings
AT gandaramartinezeleazar greensynthesisofmagneticnanoparticlesofironoxideusingaqueousextractsoflemonpeelwasteanditsapplicationinanticorrosivecoatings
AT alcortagarciaaracelia greensynthesisofmagneticnanoparticlesofironoxideusingaqueousextractsoflemonpeelwasteanditsapplicationinanticorrosivecoatings
AT martinezdelgadodorairma greensynthesisofmagneticnanoparticlesofironoxideusingaqueousextractsoflemonpeelwasteanditsapplicationinanticorrosivecoatings
AT rodriguezcastellanosedenamaral greensynthesisofmagneticnanoparticlesofironoxideusingaqueousextractsoflemonpeelwasteanditsapplicationinanticorrosivecoatings
AT vazquezrodriguezfranciscojavier greensynthesisofmagneticnanoparticlesofironoxideusingaqueousextractsoflemonpeelwasteanditsapplicationinanticorrosivecoatings
AT gomezrodriguezcristian greensynthesisofmagneticnanoparticlesofironoxideusingaqueousextractsoflemonpeelwasteanditsapplicationinanticorrosivecoatings