XPS Study on Calcining Mixtures of Brucite with Titania

In this work, we studied the phases in a Mg-Ti-O system using a 1:1 formulation of MgO:TiO2, mixing synthetic brucite of Mexican origin with TiO2 microparticles of high purity, with a heat treatment at 1100 °C for 1 h. Due to its valence electrons, TiO2 can contribute to the sintering process to imp...

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Autores principales: Sánchez Zambrano, Karla Sofía, Hernández Reséndiz, Marina, Gómez Rodríguez, Cristian, García Quiñonez, Linda Viviana, Aguilar Martínez, Josué Amilcar, Rodríguez Castellanos, Edén Amaral, Verdeja, Luis Felipe, Fernández González, Daniel, Castillo Rodríguez, Guadalupe Alan
Formato: Artículo
Lenguaje:inglés
Publicado: Molecular Diversity Preservation International 2022
Materias:
Acceso en línea:http://eprints.uanl.mx/23561/1/23561.pdf
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author Sánchez Zambrano, Karla Sofía
Hernández Reséndiz, Marina
Gómez Rodríguez, Cristian
García Quiñonez, Linda Viviana
Aguilar Martínez, Josué Amilcar
Rodríguez Castellanos, Edén Amaral
Verdeja, Luis Felipe
Fernández González, Daniel
Castillo Rodríguez, Guadalupe Alan
author_facet Sánchez Zambrano, Karla Sofía
Hernández Reséndiz, Marina
Gómez Rodríguez, Cristian
García Quiñonez, Linda Viviana
Aguilar Martínez, Josué Amilcar
Rodríguez Castellanos, Edén Amaral
Verdeja, Luis Felipe
Fernández González, Daniel
Castillo Rodríguez, Guadalupe Alan
author_sort Sánchez Zambrano, Karla Sofía
collection Repositorio Institucional
description In this work, we studied the phases in a Mg-Ti-O system using a 1:1 formulation of MgO:TiO2, mixing synthetic brucite of Mexican origin with TiO2 microparticles of high purity, with a heat treatment at 1100 °C for 1 h. Due to its valence electrons, TiO2 can contribute to the sintering process to improve density in MgO products. The raw materials and formulation by XPS and X-RD techniques were characterized. The results demonstrate the presence of different oxidation states in titania and the formation of different oxides in the Mg-Ti-O system when mixed and calcined at 1100 °C; additionally, we estimated the formation of vacancies in the crystal lattice during the transformation from hexagonal brucite to magnesia with a cubic structure centered on the faces. Its thermal behavior is indicated by the MgO-TiO2 phase diagram.
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spelling eprints-235612022-07-11T20:54:02Z http://eprints.uanl.mx/23561/ XPS Study on Calcining Mixtures of Brucite with Titania Sánchez Zambrano, Karla Sofía Hernández Reséndiz, Marina Gómez Rodríguez, Cristian García Quiñonez, Linda Viviana Aguilar Martínez, Josué Amilcar Rodríguez Castellanos, Edén Amaral Verdeja, Luis Felipe Fernández González, Daniel Castillo Rodríguez, Guadalupe Alan TA Ingeniería General y Civil In this work, we studied the phases in a Mg-Ti-O system using a 1:1 formulation of MgO:TiO2, mixing synthetic brucite of Mexican origin with TiO2 microparticles of high purity, with a heat treatment at 1100 °C for 1 h. Due to its valence electrons, TiO2 can contribute to the sintering process to improve density in MgO products. The raw materials and formulation by XPS and X-RD techniques were characterized. The results demonstrate the presence of different oxidation states in titania and the formation of different oxides in the Mg-Ti-O system when mixed and calcined at 1100 °C; additionally, we estimated the formation of vacancies in the crystal lattice during the transformation from hexagonal brucite to magnesia with a cubic structure centered on the faces. Its thermal behavior is indicated by the MgO-TiO2 phase diagram. Molecular Diversity Preservation International 2022 Article PeerReviewed text en cc_by_nc_nd http://eprints.uanl.mx/23561/1/23561.pdf http://eprints.uanl.mx/23561/1.haspreviewThumbnailVersion/23561.pdf Sánchez Zambrano, Karla Sofía y Hernández Reséndiz, Marina y Gómez Rodríguez, Cristian y García Quiñonez, Linda Viviana y Aguilar Martínez, Josué Amilcar y Rodríguez Castellanos, Edén Amaral y Verdeja, Luis Felipe y Fernández González, Daniel y Castillo Rodríguez, Guadalupe Alan (2022) XPS Study on Calcining Mixtures of Brucite with Titania. Materials, 15 (9). pp. 1-20. ISSN 1996-1944 http://doi.org/10.3390/ma15093117 doi:10.3390/ma15093117
spellingShingle TA Ingeniería General y Civil
Sánchez Zambrano, Karla Sofía
Hernández Reséndiz, Marina
Gómez Rodríguez, Cristian
García Quiñonez, Linda Viviana
Aguilar Martínez, Josué Amilcar
Rodríguez Castellanos, Edén Amaral
Verdeja, Luis Felipe
Fernández González, Daniel
Castillo Rodríguez, Guadalupe Alan
XPS Study on Calcining Mixtures of Brucite with Titania
thumbnail https://rediab.uanl.mx/themes/sandal5/images/online.png
title XPS Study on Calcining Mixtures of Brucite with Titania
title_full XPS Study on Calcining Mixtures of Brucite with Titania
title_fullStr XPS Study on Calcining Mixtures of Brucite with Titania
title_full_unstemmed XPS Study on Calcining Mixtures of Brucite with Titania
title_short XPS Study on Calcining Mixtures of Brucite with Titania
title_sort xps study on calcining mixtures of brucite with titania
topic TA Ingeniería General y Civil
url http://eprints.uanl.mx/23561/1/23561.pdf
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