Sequential Nucleation Growth of ZnO Nanoflowers

The morphological characteristics of ZnO nanostructures were systematically studied from dense rods to flower-like shapes. The ZnO flower-like samples were prepared by direct decomposition of a Zn(OH)4 2– precursor and by the sequential nucleation and growth method consisted of a multistep synthesis...

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Autores principales: Elizondo V., Nora, Martínez Delgado, Dora Irma, Arato Tovar, Ana María, González López, Rodrigo, Vázquez Rodríguez, Francisco Javier, Rodríguez, Gustavo, Torres López, Ernesto, Castaño Meneses, Víctor Manuel
Formato: Artículo
Lenguaje:Spanish / Castilian
Publicado: Open-Access House of Science and Technology 2018
Materias:
Acceso en línea:http://eprints.uanl.mx/22396/1/2018-Sequential%20Nucleation%20Growth%20of%20ZnO%20Nanoflowers-%20Nanobiomedicine.pdf
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author Elizondo V., Nora
Martínez Delgado, Dora Irma
Arato Tovar, Ana María
González López, Rodrigo
Vázquez Rodríguez, Francisco Javier
Rodríguez, Gustavo
Torres López, Ernesto
Castaño Meneses, Víctor Manuel
author_facet Elizondo V., Nora
Martínez Delgado, Dora Irma
Arato Tovar, Ana María
González López, Rodrigo
Vázquez Rodríguez, Francisco Javier
Rodríguez, Gustavo
Torres López, Ernesto
Castaño Meneses, Víctor Manuel
author_sort Elizondo V., Nora
collection Repositorio Institucional
description The morphological characteristics of ZnO nanostructures were systematically studied from dense rods to flower-like shapes. The ZnO flower-like samples were prepared by direct decomposition of a Zn(OH)4 2– precursor and by the sequential nucleation and growth method consisted of a multistep synthesis of complex nanostructured films. Condition-dependent experiments systematically were compared as to reveal the formation and detailed growth process of ZnO nanosized crystallites and aggregates. X-ray diffraction, transmission and scanning electron microscopy indicated that the precursor, solution basicity, reaction temperature and pressure as well as reaction time, were responsible for the variations of the morphologies. ZnO flower-like and large nanorods of exceptional uniformity, orientation alignment, and optical properties have been produced in this work. Several synthesis steps are needed to produce oriented nanostructures that are more complex than simple nanorod architectures. These structures have potential applications in building functional electronics devices and optoelectronic properties.
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spelling eprints-223962024-03-04T17:36:46Z http://eprints.uanl.mx/22396/ Sequential Nucleation Growth of ZnO Nanoflowers Elizondo V., Nora Martínez Delgado, Dora Irma Arato Tovar, Ana María González López, Rodrigo Vázquez Rodríguez, Francisco Javier Rodríguez, Gustavo Torres López, Ernesto Castaño Meneses, Víctor Manuel TP Tecnología Química The morphological characteristics of ZnO nanostructures were systematically studied from dense rods to flower-like shapes. The ZnO flower-like samples were prepared by direct decomposition of a Zn(OH)4 2– precursor and by the sequential nucleation and growth method consisted of a multistep synthesis of complex nanostructured films. Condition-dependent experiments systematically were compared as to reveal the formation and detailed growth process of ZnO nanosized crystallites and aggregates. X-ray diffraction, transmission and scanning electron microscopy indicated that the precursor, solution basicity, reaction temperature and pressure as well as reaction time, were responsible for the variations of the morphologies. ZnO flower-like and large nanorods of exceptional uniformity, orientation alignment, and optical properties have been produced in this work. Several synthesis steps are needed to produce oriented nanostructures that are more complex than simple nanorod architectures. These structures have potential applications in building functional electronics devices and optoelectronic properties. Open-Access House of Science and Technology 2018 Article PeerReviewed text es cc_by_nc_nd http://eprints.uanl.mx/22396/1/2018-Sequential%20Nucleation%20Growth%20of%20ZnO%20Nanoflowers-%20Nanobiomedicine.pdf http://eprints.uanl.mx/22396/1.haspreviewThumbnailVersion/2018-Sequential%20Nucleation%20Growth%20of%20ZnO%20Nanoflowers-%20Nanobiomedicine.pdf Elizondo V., Nora y Martínez Delgado, Dora Irma y Arato Tovar, Ana María y González López, Rodrigo y Vázquez Rodríguez, Francisco Javier y Rodríguez, Gustavo y Torres López, Ernesto y Castaño Meneses, Víctor Manuel (2018) Sequential Nucleation Growth of ZnO Nanoflowers. Nano Biomed. Eng., 10 (1). pp. 87-95. ISSN 2150-5578
spellingShingle TP Tecnología Química
Elizondo V., Nora
Martínez Delgado, Dora Irma
Arato Tovar, Ana María
González López, Rodrigo
Vázquez Rodríguez, Francisco Javier
Rodríguez, Gustavo
Torres López, Ernesto
Castaño Meneses, Víctor Manuel
Sequential Nucleation Growth of ZnO Nanoflowers
thumbnail https://rediab.uanl.mx/themes/sandal5/images/online.png
title Sequential Nucleation Growth of ZnO Nanoflowers
title_full Sequential Nucleation Growth of ZnO Nanoflowers
title_fullStr Sequential Nucleation Growth of ZnO Nanoflowers
title_full_unstemmed Sequential Nucleation Growth of ZnO Nanoflowers
title_short Sequential Nucleation Growth of ZnO Nanoflowers
title_sort sequential nucleation growth of zno nanoflowers
topic TP Tecnología Química
url http://eprints.uanl.mx/22396/1/2018-Sequential%20Nucleation%20Growth%20of%20ZnO%20Nanoflowers-%20Nanobiomedicine.pdf
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