Photocatalytic Performance of Titanates with Formula MTiO3 (M= Fe, Ni, and Co) Synthesized by Solvo-Combustion Method

This work reports the synthesis of a variety of materials with an ilmenite-type structure MTiO3 formula, where M= Fe, Co, and Ni, these materials were synthesized by the method of solvo-combustion, a simple and rapid method. These materials were characterized by X-ray Diffraction (XRD), scanning ele...

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Main Authors: Zarazúa Morín, María Elvira, Torres Martínez, Leticia Myriam, Sánchez Martínez, Daniel, Gómez Solís, Christian
Format: Article
Language:English
Published: Universidade Federal de São Carlos 2017
Subjects:
Online Access:http://eprints.uanl.mx/17532/1/325.pdf
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author Zarazúa Morín, María Elvira
Torres Martínez, Leticia Myriam
Sánchez Martínez, Daniel
Gómez Solís, Christian
author_facet Zarazúa Morín, María Elvira
Torres Martínez, Leticia Myriam
Sánchez Martínez, Daniel
Gómez Solís, Christian
author_sort Zarazúa Morín, María Elvira
collection Repositorio Institucional
description This work reports the synthesis of a variety of materials with an ilmenite-type structure MTiO3 formula, where M= Fe, Co, and Ni, these materials were synthesized by the method of solvo-combustion, a simple and rapid method. These materials were characterized by X-ray Diffraction (XRD), scanning electron microscopy (SEM), FT-IR spectroscopy, thermogravimetric analysis (TGA/DTA), surface area determination by the BET method and analysis of particle size. The photocatalytic activity was measured in the degradation reactions of Rhodamine B (rhB) and tetracycline (TC). The results show that the crystallinity and surface area are factors that influence significantly on the photocatalytic activity of the synthesized titanates. Keywords: Non-aqueous solution, Characterization, Titanates, solvo-combustion, organic pollutants, photocatalysis
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spelling eprints-175322025-07-14T16:28:45Z http://eprints.uanl.mx/17532/ Photocatalytic Performance of Titanates with Formula MTiO3 (M= Fe, Ni, and Co) Synthesized by Solvo-Combustion Method Zarazúa Morín, María Elvira Torres Martínez, Leticia Myriam Sánchez Martínez, Daniel Gómez Solís, Christian TA Ingeniería General y Civil This work reports the synthesis of a variety of materials with an ilmenite-type structure MTiO3 formula, where M= Fe, Co, and Ni, these materials were synthesized by the method of solvo-combustion, a simple and rapid method. These materials were characterized by X-ray Diffraction (XRD), scanning electron microscopy (SEM), FT-IR spectroscopy, thermogravimetric analysis (TGA/DTA), surface area determination by the BET method and analysis of particle size. The photocatalytic activity was measured in the degradation reactions of Rhodamine B (rhB) and tetracycline (TC). The results show that the crystallinity and surface area are factors that influence significantly on the photocatalytic activity of the synthesized titanates. Keywords: Non-aqueous solution, Characterization, Titanates, solvo-combustion, organic pollutants, photocatalysis Universidade Federal de São Carlos 2017-07-03 Article PeerReviewed text en cc_by_nc_nd http://eprints.uanl.mx/17532/1/325.pdf http://eprints.uanl.mx/17532/1.haspreviewThumbnailVersion/325.pdf Zarazúa Morín, María Elvira y Torres Martínez, Leticia Myriam y Sánchez Martínez, Daniel y Gómez Solís, Christian (2017) Photocatalytic Performance of Titanates with Formula MTiO3 (M= Fe, Ni, and Co) Synthesized by Solvo-Combustion Method. Materials Research, 20 (5). pp. 1322-1331. ISSN 1516-1439 http://doi.org/10.1590/1980-5373-MR-2016-0615 doi:10.1590/1980-5373-MR-2016-0615
spellingShingle TA Ingeniería General y Civil
Zarazúa Morín, María Elvira
Torres Martínez, Leticia Myriam
Sánchez Martínez, Daniel
Gómez Solís, Christian
Photocatalytic Performance of Titanates with Formula MTiO3 (M= Fe, Ni, and Co) Synthesized by Solvo-Combustion Method
thumbnail https://rediab.uanl.mx/themes/sandal5/images/online.png
title Photocatalytic Performance of Titanates with Formula MTiO3 (M= Fe, Ni, and Co) Synthesized by Solvo-Combustion Method
title_full Photocatalytic Performance of Titanates with Formula MTiO3 (M= Fe, Ni, and Co) Synthesized by Solvo-Combustion Method
title_fullStr Photocatalytic Performance of Titanates with Formula MTiO3 (M= Fe, Ni, and Co) Synthesized by Solvo-Combustion Method
title_full_unstemmed Photocatalytic Performance of Titanates with Formula MTiO3 (M= Fe, Ni, and Co) Synthesized by Solvo-Combustion Method
title_short Photocatalytic Performance of Titanates with Formula MTiO3 (M= Fe, Ni, and Co) Synthesized by Solvo-Combustion Method
title_sort photocatalytic performance of titanates with formula mtio3 m fe ni and co synthesized by solvo combustion method
topic TA Ingeniería General y Civil
url http://eprints.uanl.mx/17532/1/325.pdf
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AT torresmartinezleticiamyriam photocatalyticperformanceoftitanateswithformulamtio3mfeniandcosynthesizedbysolvocombustionmethod
AT sanchezmartinezdaniel photocatalyticperformanceoftitanateswithformulamtio3mfeniandcosynthesizedbysolvocombustionmethod
AT gomezsolischristian photocatalyticperformanceoftitanateswithformulamtio3mfeniandcosynthesizedbysolvocombustionmethod