Pb(core)/ZnO(shell) nanowires obtained by microwave-assisted method
In this study, Pb-filled ZnO nanowires [Pb(core)/ZnO(shell)] were synthesized by a simple and novel one-step vapor transport and condensation method by microwave-assisted decomposition of zinc ferrite. The synthesis was performed using a conventional oven at 1000 W and 5 min of treatment. After synt...
| Autores principales: | , , , |
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| Formato: | Artículo |
| Lenguaje: | inglés |
| Publicado: |
Springer
2011
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| Materias: | |
| Acceso en línea: | http://eprints.uanl.mx/15053/1/670.pdf |
| _version_ | 1824414239812485120 |
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| author | Solís Pomar, Francisco Meléndrez, Manuel F. Esparza, Rodrigo Pérez Tijerina, Eduardo |
| author_facet | Solís Pomar, Francisco Meléndrez, Manuel F. Esparza, Rodrigo Pérez Tijerina, Eduardo |
| author_sort | Solís Pomar, Francisco |
| collection | Repositorio Institucional |
| description | In this study, Pb-filled ZnO nanowires [Pb(core)/ZnO(shell)] were synthesized by a simple and novel one-step vapor transport and condensation method by microwave-assisted decomposition of zinc ferrite. The synthesis was performed using a conventional oven at 1000 W and 5 min of treatment. After synthesis, a spongy white cottonlike material was obtained in the condensation zone of the reaction system. HRTEM analysis revealed that product consists of a Pb-(core) with (fcc) cubic structure that preferentially grows in the [111] direction and a hexagonal wurtzite ZnO-(Shell) that grows in the [001] direction. Nanowire length was more than 5 μm and a statistical analysis determined that the shell and core diameters were 21.00 ± 3.00 and 4.00 ± 1.00 nm, respectively. Experimental, structural details, and synthesis mechanism are discussed in this study |
| format | Article |
| id | eprints-15053 |
| institution | UANL |
| language | English |
| publishDate | 2011 |
| publisher | Springer |
| record_format | eprints |
| spelling | eprints-150532020-10-01T18:17:16Z http://eprints.uanl.mx/15053/ Pb(core)/ZnO(shell) nanowires obtained by microwave-assisted method Solís Pomar, Francisco Meléndrez, Manuel F. Esparza, Rodrigo Pérez Tijerina, Eduardo TK Ingeniería Eléctrica, Electrónica, Ingeniería Nuclear In this study, Pb-filled ZnO nanowires [Pb(core)/ZnO(shell)] were synthesized by a simple and novel one-step vapor transport and condensation method by microwave-assisted decomposition of zinc ferrite. The synthesis was performed using a conventional oven at 1000 W and 5 min of treatment. After synthesis, a spongy white cottonlike material was obtained in the condensation zone of the reaction system. HRTEM analysis revealed that product consists of a Pb-(core) with (fcc) cubic structure that preferentially grows in the [111] direction and a hexagonal wurtzite ZnO-(Shell) that grows in the [001] direction. Nanowire length was more than 5 μm and a statistical analysis determined that the shell and core diameters were 21.00 ± 3.00 and 4.00 ± 1.00 nm, respectively. Experimental, structural details, and synthesis mechanism are discussed in this study Springer 2011 Article PeerReviewed text en cc_by_nc_nd http://eprints.uanl.mx/15053/1/670.pdf http://eprints.uanl.mx/15053/1.haspreviewThumbnailVersion/670.pdf Solís Pomar, Francisco y Meléndrez, Manuel F. y Esparza, Rodrigo y Pérez Tijerina, Eduardo (2011) Pb(core)/ZnO(shell) nanowires obtained by microwave-assisted method. Nanoscale research letters, 6 (1). p. 553. ISSN 1931-7573 http://doi.org/10.1186/1556-276X-6-553 doi:10.1186/1556-276X-6-553 |
| spellingShingle | TK Ingeniería Eléctrica, Electrónica, Ingeniería Nuclear Solís Pomar, Francisco Meléndrez, Manuel F. Esparza, Rodrigo Pérez Tijerina, Eduardo Pb(core)/ZnO(shell) nanowires obtained by microwave-assisted method |
| thumbnail | https://rediab.uanl.mx/themes/sandal5/images/online.png |
| title | Pb(core)/ZnO(shell) nanowires obtained by microwave-assisted method |
| title_full | Pb(core)/ZnO(shell) nanowires obtained by microwave-assisted method |
| title_fullStr | Pb(core)/ZnO(shell) nanowires obtained by microwave-assisted method |
| title_full_unstemmed | Pb(core)/ZnO(shell) nanowires obtained by microwave-assisted method |
| title_short | Pb(core)/ZnO(shell) nanowires obtained by microwave-assisted method |
| title_sort | pb core zno shell nanowires obtained by microwave assisted method |
| topic | TK Ingeniería Eléctrica, Electrónica, Ingeniería Nuclear |
| url | http://eprints.uanl.mx/15053/1/670.pdf |
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