Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description
The aim of this work is to present some results of the synthesis of nanoparticles of zinc oxide by means of a hydrothermal method. Also, a description of the structural characteristics of these nanoparticles will be presented. The nanoparticles can be used as the supported active phase for photocata...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | Spanish / Castilian |
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Universidad Autónoma de Puebla
2011
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| Online Access: | http://eprints.uanl.mx/13445/1/Art5.pdf |
| _version_ | 1824413711344861184 |
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| author | García Ruiz, Armando Escobedo, A. Aguilar Hernández, Alberto Issac Esparza, Rodrigo Pérez, R. |
| author_facet | García Ruiz, Armando Escobedo, A. Aguilar Hernández, Alberto Issac Esparza, Rodrigo Pérez, R. |
| author_sort | García Ruiz, Armando |
| collection | Repositorio Institucional |
| description | The aim of this work is to present some results of the synthesis of nanoparticles of zinc oxide by means of a hydrothermal method. Also, a description of the structural characteristics of these nanoparticles will be presented. The nanoparticles can be used as the supported active phase for photocatalytic applications, as has been recently published in the literature. The hydrothermal synthesis is based in dehydrated zinc acetate as the precursor using temperatures of 100ºC. The structural analysis of the obtained nanoparticles has been performed using X-ray diffraction techniques with a subsequent Rietveld refinement of the pattern. This allows obtaining refined values of the cell parameters and the aproximate crystallite sizes (10-20 nm) and also gives an insight on the morphology of the nanoparticle (truncated cube). Some high resolution electron microscope images are also presented and their structural results are compared with those obtained through the X-ray diffraction stuides. |
| format | Article |
| id | eprints-13445 |
| institution | UANL |
| language | Spanish / Castilian |
| publishDate | 2011 |
| publisher | Universidad Autónoma de Puebla |
| record_format | eprints |
| spelling | eprints-134452020-04-28T17:43:42Z http://eprints.uanl.mx/13445/ Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description García Ruiz, Armando Escobedo, A. Aguilar Hernández, Alberto Issac Esparza, Rodrigo Pérez, R. QD Química The aim of this work is to present some results of the synthesis of nanoparticles of zinc oxide by means of a hydrothermal method. Also, a description of the structural characteristics of these nanoparticles will be presented. The nanoparticles can be used as the supported active phase for photocatalytic applications, as has been recently published in the literature. The hydrothermal synthesis is based in dehydrated zinc acetate as the precursor using temperatures of 100ºC. The structural analysis of the obtained nanoparticles has been performed using X-ray diffraction techniques with a subsequent Rietveld refinement of the pattern. This allows obtaining refined values of the cell parameters and the aproximate crystallite sizes (10-20 nm) and also gives an insight on the morphology of the nanoparticle (truncated cube). Some high resolution electron microscope images are also presented and their structural results are compared with those obtained through the X-ray diffraction stuides. Universidad Autónoma de Puebla 2011-09-10 Article PeerReviewed text es cc_by_nc_nd http://eprints.uanl.mx/13445/1/Art5.pdf http://eprints.uanl.mx/13445/1.haspreviewThumbnailVersion/Art5.pdf García Ruiz, Armando y Escobedo, A. y Aguilar Hernández, Alberto Issac y Esparza, Rodrigo y Pérez, R. (2011) Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description. Química Hoy, 1 (4). pp. 24-28. ISSN 2007-1183 |
| spellingShingle | QD Química García Ruiz, Armando Escobedo, A. Aguilar Hernández, Alberto Issac Esparza, Rodrigo Pérez, R. Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description |
| thumbnail | https://rediab.uanl.mx/themes/sandal5/images/online.png |
| title | Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description |
| title_full | Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description |
| title_fullStr | Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description |
| title_full_unstemmed | Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description |
| title_short | Hydrothermally synthesized nanoparticles of zinc peroxide and their structural description |
| title_sort | hydrothermally synthesized nanoparticles of zinc peroxide and their structural description |
| topic | QD Química |
| url | http://eprints.uanl.mx/13445/1/Art5.pdf |
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