Synthesis of high purity -SiC and -Si3N4 from rice hulls
Silicon carbide and silicon nitride were synthesized from ashes obtained by heating rice hulls at 800ºC for 3 hours in argon. -SiC was produced from the ashes by reheating them at 1400ºC for 8 hours in argon, whereas -Si3N4 was obtained by heating the ashes at temperatures ranging from 1250 to 1400º...
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Format: | Article |
Language: | English |
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Universidad Autónoma de Nuevo León
2011
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Online Access: | http://eprints.uanl.mx/13370/1/Art8.pdf |
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author | Treviño, B. Gómez de la Fuente, María Idalia del Consuelo Colás Ortíz, Rafael |
author_facet | Treviño, B. Gómez de la Fuente, María Idalia del Consuelo Colás Ortíz, Rafael |
author_sort | Treviño, B. |
collection | Repositorio Institucional |
description | Silicon carbide and silicon nitride were synthesized from ashes obtained by heating rice hulls at 800ºC for 3 hours in argon. -SiC was produced from the ashes by reheating them at 1400ºC for 8 hours in argon, whereas -Si3N4 was obtained by heating the ashes at temperatures ranging from 1250 to 1400ºC for periods of 3 to 6 hours in a nitrogen rich atmosphere. The products were characterized by infrared spectroscopy, X-ray and scanning electron microscopy. High purity -SiC and -Si3N4 compouds with whisker type morphology were obtained. It was possible to obtain -Si3N4 without -SiC by heating the ashes for 6 hours at 1250ºC |
format | Article |
id | eprints-13370 |
institution | UANL |
language | English |
publishDate | 2011 |
publisher | Universidad Autónoma de Nuevo León |
record_format | eprints |
spelling | eprints-133702025-06-27T18:27:29Z http://eprints.uanl.mx/13370/ Synthesis of high purity -SiC and -Si3N4 from rice hulls Treviño, B. Gómez de la Fuente, María Idalia del Consuelo Colás Ortíz, Rafael QD Química Silicon carbide and silicon nitride were synthesized from ashes obtained by heating rice hulls at 800ºC for 3 hours in argon. -SiC was produced from the ashes by reheating them at 1400ºC for 8 hours in argon, whereas -Si3N4 was obtained by heating the ashes at temperatures ranging from 1250 to 1400ºC for periods of 3 to 6 hours in a nitrogen rich atmosphere. The products were characterized by infrared spectroscopy, X-ray and scanning electron microscopy. High purity -SiC and -Si3N4 compouds with whisker type morphology were obtained. It was possible to obtain -Si3N4 without -SiC by heating the ashes for 6 hours at 1250ºC Universidad Autónoma de Nuevo León 2011-06-10 Article PeerReviewed text en cc_by_nc_nd http://eprints.uanl.mx/13370/1/Art8.pdf http://eprints.uanl.mx/13370/1.haspreviewThumbnailVersion/Art8.pdf Treviño, B. y Gómez de la Fuente, María Idalia del Consuelo y Colás Ortíz, Rafael (2011) Synthesis of high purity -SiC and -Si3N4 from rice hulls. Química Hoy, 1 (3). pp. 34-40. ISSN 2007-1183 |
spellingShingle | QD Química Treviño, B. Gómez de la Fuente, María Idalia del Consuelo Colás Ortíz, Rafael Synthesis of high purity -SiC and -Si3N4 from rice hulls |
thumbnail | https://rediab.uanl.mx/themes/sandal5/images/online.png |
title | Synthesis of high purity -SiC and -Si3N4 from rice hulls |
title_full | Synthesis of high purity -SiC and -Si3N4 from rice hulls |
title_fullStr | Synthesis of high purity -SiC and -Si3N4 from rice hulls |
title_full_unstemmed | Synthesis of high purity -SiC and -Si3N4 from rice hulls |
title_short | Synthesis of high purity -SiC and -Si3N4 from rice hulls |
title_sort | synthesis of high purity sic and si3n4 from rice hulls |
topic | QD Química |
url | http://eprints.uanl.mx/13370/1/Art8.pdf |
work_keys_str_mv | AT trevinob synthesisofhighpuritysicandsi3n4fromricehulls AT gomezdelafuentemariaidaliadelconsuelo synthesisofhighpuritysicandsi3n4fromricehulls AT colasortizrafael synthesisofhighpuritysicandsi3n4fromricehulls |